Micromeritics Instrument Corp. MicroActive 3.00 Gemini VII 2390 V1.03 Page 1 Serial # 674 Unit 1 Sample: gvmh97400 Operator: manohara Submitter: degas 100 File: C:\Gemini VII\data\USERS\Manohara\gvmh97.SMP Started: 20/07/2020 15:17:42 Analysis adsorptive: N2 Completed: 20/07/2020 21:54:54 Equilibration time: 10 s Report time: 21/07/2020 12:10:01 Sat. pressure: 770.761 mmHg Sample mass: 0.1210 g Free space diff.: 0.0451 cm³ Free space type: Measured Sample density: 1.000 g/cm³ Evac. rate: 20.0 mmHg/min Gemini model: 2390 a Summary Report Surface Area Single point surface area at p/p° = 0.303686652: 158.8018 m²/g BET Surface Area: 162.4547 m²/g Pore Volume Single point desorption total pore volume of pores less than -1.#IND nm diameter at p/p° = -1.000000000: 0.000000 cm³/g Pore Size Desorption average pore diameter (4V/A by BET): 0.00000 nm Micromeritics Instrument Corp. MicroActive 3.00 Gemini VII 2390 V1.03 Page 1 Serial # 674 Unit 1 Sample: gvmh97400 Operator: manohara Submitter: degas 100 File: C:\Gemini VII\data\USERS\Manohara\gvmh97.SMP Started: 20/07/2020 15:17:42 Analysis adsorptive: N2 Completed: 20/07/2020 21:54:54 Equilibration time: 10 s Report time: 21/07/2020 12:10:01 Sat. pressure: 770.761 mmHg Sample mass: 0.1210 g Free space diff.: 0.0451 cm³ Free space type: Measured Sample density: 1.000 g/cm³ Evac. rate: 20.0 mmHg/min Gemini model: 2390 a Isotherm Tabular Report Relative Absolute Quantity Elapsed Saturation Pressure Pressure Adsorbed Time Pressure (p/p°) (mmHg) (mmol/g) (h:min) (mmHg) ----- 770.761292 0.004850987 3.738953 1.03939 02:11 0.049878494 38.444412 1.61717 02:17 0.054652564 42.124081 1.64081 02:21 0.075019116 57.821831 1.72477 02:25 0.099898714 76.998062 1.81079 02:30 0.104493587 80.539612 1.82531 02:33 0.124772255 96.169624 1.88570 02:38 0.149869185 115.513367 1.95456 02:42 0.154046251 118.732887 1.96528 02:45 0.174956128 134.849411 2.01887 02:49 0.200036518 154.180405 2.08163 02:53 0.203975633 157.216522 2.09171 02:56 0.225044906 173.455902 2.14222 03:00 0.250224479 192.863342 2.20501 03:04 0.254147241 195.886856 2.21547 03:07 0.303686652 234.069916 2.33767 03:12 0.353541725 272.496277 2.46441 03:17 0.403303714 310.850891 2.59615 03:22 0.453039649 349.185425 2.73472 03:28 0.502699207 387.461090 2.88179 03:33 0.552499958 425.845581 3.04076 03:39 0.602119368 464.090302 3.21703 03:46 0.651517249 502.164276 3.41879 03:53 0.701228279 540.479614 3.66798 04:00 0.750901894 578.766113 3.99986 04:10 0.800828672 617.247742 4.47941 04:23 0.850601272 655.610535 5.26374 04:44 0.900174238 693.819458 6.68660 05:20 0.949882695 732.132813 10.37950 06:36 Micromeritics Instrument Corp. MicroActive 3.00 Gemini VII 2390 V1.03 Page 1 Serial # 674 Unit 1 Sample: gvmh97400 Operator: manohara Submitter: degas 100 File: C:\Gemini VII\data\USERS\Manohara\gvmh97.SMP Started: 20/07/2020 15:17:42 Analysis adsorptive: N2 Completed: 20/07/2020 21:54:54 Equilibration time: 10 s Report time: 21/07/2020 12:10:01 Sat. pressure: 770.761 mmHg Sample mass: 0.1210 g Free space diff.: 0.0451 cm³ Free space type: Measured Sample density: 1.000 g/cm³ Evac. rate: 20.0 mmHg/min Gemini model: 2390 a Isotherm Linear Plot gvmh97400 - Adsorption Relative Pressure (p/p°) Quantity Adsorbed (mmol/g) 0.00485099 1.03939 0.0498785 1.61717 0.0546526 1.64081 0.0750191 1.72477 0.0998987 1.81079 0.104494 1.82531 0.124772 1.8857 0.149869 1.95456 0.154046 1.96528 0.174956 2.01887 0.200037 2.08163 0.203976 2.09171 0.225045 2.14222 0.250224 2.20501 0.254147 2.21547 0.303687 2.33767 0.353542 2.46441 0.403304 2.59615 0.45304 2.73472 0.502699 2.88179 0.5525 3.04076 0.602119 3.21703 0.651517 3.41879 0.701228 3.66798 0.750902 3.99986 0.800829 4.47941 0.850601 5.26374 0.900174 6.6866 0.949883 10.3795 Micromeritics Instrument Corp. MicroActive 3.00 Gemini VII 2390 V1.03 Page 1 Serial # 674 Unit 1 Sample: gvmh97400 Operator: manohara Submitter: degas 100 File: C:\Gemini VII\data\USERS\Manohara\gvmh97.SMP Started: 20/07/2020 15:17:42 Analysis adsorptive: N2 Completed: 20/07/2020 21:54:54 Equilibration time: 10 s Report time: 21/07/2020 12:10:01 Sat. pressure: 770.761 mmHg Sample mass: 0.1210 g Free space diff.: 0.0451 cm³ Free space type: Measured Sample density: 1.000 g/cm³ Evac. rate: 20.0 mmHg/min Gemini model: 2390 a BET Report BET surface area: 162.4547 ± 1.0095 m²/g Slope: 0.599131 ± 0.003677 g/mmol Y-intercept: 0.001400 ± 0.000634 g/mmol C: 428.805315 Qm: 1.66519 mmol/g Correlation coefficient: 0.9997364 Molecular cross-sectional area: 0.1620 nm² Relative Quantity Pressure Adsorbed 1/[Q(p°/p (p/p°) (mmol/g) - 1)] --- 0.004850987 1.03939 0.00469 0.049878494 1.61717 0.03246 0.054652564 1.64081 0.03523 0.075019116 1.72477 0.04702 0.099898714 1.81079 0.06129 0.104493587 1.82531 0.06393 0.124772255 1.88570 0.07560 0.149869185 1.95456 0.09019 0.154046251 1.96528 0.09266 0.174956128 2.01887 0.10504 0.200036518 2.08163 0.12013 0.203975633 2.09171 0.12250 0.225044906 2.14222 0.13556 0.250224479 2.20501 0.15135 0.254147241 2.21547 0.15380 0.303686652 2.33767 0.18657 Micromeritics Instrument Corp. MicroActive 3.00 Gemini VII 2390 V1.03 Page 1 Serial # 674 Unit 1 Sample: gvmh97400 Operator: manohara Submitter: degas 100 File: C:\Gemini VII\data\USERS\Manohara\gvmh97.SMP Started: 20/07/2020 15:17:42 Analysis adsorptive: N2 Completed: 20/07/2020 21:54:54 Equilibration time: 10 s Report time: 21/07/2020 12:10:01 Sat. pressure: 770.761 mmHg Sample mass: 0.1210 g Free space diff.: 0.0451 cm³ Free space type: Measured Sample density: 1.000 g/cm³ Evac. rate: 20.0 mmHg/min Gemini model: 2390 a BET Surface Area Plot gvmh97400 Relative Pressure (p/p°) 1/[Q(p°/p - 1)] 0.00485099 0.00468988 0.0498785 0.0324622 0.0546526 0.0352339 0.0750191 0.0470226 0.0998987 0.0612914 0.104494 0.0639269 0.124772 0.0756003 0.149869 0.090194 0.154046 0.0926573 0.174956 0.105037 0.200037 0.120125 0.203976 0.122504 0.225045 0.135559 0.250224 0.151352 0.254147 0.153803 0.303687 0.186568 Not Fitted Relative Pressure (p/p°) 1/[Q(p°/p - 1)] Micromeritics Instrument Corp. MicroActive 3.00 Gemini VII 2390 V1.03 Page 1 Serial # 674 Unit 1 Sample: gvmh97400 Operator: manohara Submitter: degas 100 File: C:\Gemini VII\data\USERS\Manohara\gvmh97.SMP Started: 20/07/2020 15:17:42 Analysis adsorptive: N2 Completed: 20/07/2020 21:54:54 Equilibration time: 10 s Report time: 21/07/2020 12:10:01 Sat. pressure: 770.761 mmHg Sample mass: 0.1210 g Free space diff.: 0.0451 cm³ Free space type: Measured Sample density: 1.000 g/cm³ Evac. rate: 20.0 mmHg/min Gemini model: 2390 a Langmuir Reports Primary Data At least two points must be selected for this calculation. Primary Data At least two points must be selected for this calculation. Micromeritics Instrument Corp. MicroActive 3.00 Gemini VII 2390 V1.03 Page 1 Serial # 674 Unit 1 Sample: gvmh97400 Operator: manohara Submitter: degas 100 File: C:\Gemini VII\data\USERS\Manohara\gvmh97.SMP Started: 20/07/2020 15:17:42 Analysis adsorptive: N2 Completed: 20/07/2020 21:54:54 Equilibration time: 10 s Report time: 21/07/2020 12:10:01 Sat. pressure: 770.761 mmHg Sample mass: 0.1210 g Free space diff.: 0.0451 cm³ Free space type: Measured Sample density: 1.000 g/cm³ Evac. rate: 20.0 mmHg/min Gemini model: 2390 a t-Plot Reports Primary Data 4053- At least two data points must be selected for t-Plot calculations. Micromeritics Instrument Corp. MicroActive 3.00 Gemini VII 2390 V1.03 Page 1 Serial # 674 Unit 1 Sample: gvmh97400 Operator: manohara Submitter: degas 100 File: C:\Gemini VII\data\USERS\Manohara\gvmh97.SMP Started: 20/07/2020 15:17:42 Analysis adsorptive: N2 Completed: 20/07/2020 21:54:54 Equilibration time: 10 s Report time: 21/07/2020 12:10:01 Sat. pressure: 770.761 mmHg Sample mass: 0.1210 g Free space diff.: 0.0451 cm³ Free space type: Measured Sample density: 1.000 g/cm³ Evac. rate: 20.0 mmHg/min Gemini model: 2390 a BJH Desorption Reports Primary Data 1043- Fewer than 2 points available for BJH Desorption calculations. Micromeritics Instrument Corp. MicroActive 3.00 Gemini VII 2390 V1.03 Page 1 Serial # 674 Unit 1 Sample: gvmh97400 Operator: manohara Submitter: degas 100 File: C:\Gemini VII\data\USERS\Manohara\gvmh97.SMP Started: 20/07/2020 15:17:42 Analysis adsorptive: N2 Completed: 20/07/2020 21:54:54 Equilibration time: 10 s Report time: 21/07/2020 12:10:01 Sat. pressure: 770.761 mmHg Sample mass: 0.1210 g Free space diff.: 0.0451 cm³ Free space type: Measured Sample density: 1.000 g/cm³ Evac. rate: 20.0 mmHg/min Gemini model: 2390 a DFT Pore Size Reports Primary Data 4073- The analysis gas (N2) does not match the model gas (AR).